Quantitative Analysis
CHXI12:ORGANIC CHEMISTRY SOME BASIC PRINCIPLES AND TECHNIQUES

317522 In Dumas method for the estimation of \(\mathrm{N}_{2}\), the sample is heated with copper oxide and the gas evolved is passed over

1 Copper gauze
2 Pd
3 Ni
4 Copper oxide
CHXI12:ORGANIC CHEMISTRY SOME BASIC PRINCIPLES AND TECHNIQUES

317523 \(0.257 \mathrm{~g}\) of an organic substance was heated with conc \(\mathrm{H}_{2} \mathrm{SO}_{4}\) and then distilled with excess of strong alkali. The ammonia gas evolved was absorbed in \({\rm{50}}\,\,{\rm{ml}}\) of \({\rm{N/10}}\,{\rm{HCl}}\) which required \({\rm{23}}{\rm{.2}}\,\,{\rm{ml}}\) of \({\rm{N/10}}\,\,{\rm{NaOH}}\) for neutralisation at the end of the process. The percentage of nitrogen in the compound is-

1 14.6
2 18.0
3 17.0
4 15.5
CHXI12:ORGANIC CHEMISTRY SOME BASIC PRINCIPLES AND TECHNIQUES

317524 Assertion :
The Duma's method is more appicable to nitrogen containing organic compounds than the Kjeldahl's method.
Reason :
The Kjeldahl's method does not give satisfactory results for compounds in which nitrogen is directly linked to oxygen.

1 Both Assertion and Reason are correct and Reason is the correct explanation of the Assertion.
2 Both Assertion and Reason are correct but Reason is not the correct explanation of the Assertion.
3 Assertion is correct but Reason is incorrect.
4 Assertion is incorrect but Reason is correct.
CHXI12:ORGANIC CHEMISTRY SOME BASIC PRINCIPLES AND TECHNIQUES

317525 During estimation of nitrogen present in an organic compound by Kjeldahl's method, the ammonia evolved from 0.5 g of the compound in Kjeldahl's estimation of nitrogen, neutralized 10 mL of \(1 \mathrm{M} \,\mathrm{H}_{2} \mathrm{SO}_{4}\). Find out the percentage of nitrogen in the compound.

1 \(53 \%\)
2 \(58 \%\)
3 \(56 \%\)
4 \(52 \%\)
CHXI12:ORGANIC CHEMISTRY SOME BASIC PRINCIPLES AND TECHNIQUES

317526 In Kjeldahl's method for the estimation of \(\mathrm{N}_{2}\), potassium sulphate and copper sulphate are used. On the basis of their functions which of the following statement(s) is/are correct?
(I) Potassium sulphate raises the b.pt. and ensures complete reaction.
(II) Copper sulphate acts as catalyst.
(III)Potassium sulphate acts as catalyst and copper sulphate raises the b.pt.

1 Only (III) is correct
2 (I) and (II) are correct
3 Only (II) is correct
4 None is correct
CHXI12:ORGANIC CHEMISTRY SOME BASIC PRINCIPLES AND TECHNIQUES

317522 In Dumas method for the estimation of \(\mathrm{N}_{2}\), the sample is heated with copper oxide and the gas evolved is passed over

1 Copper gauze
2 Pd
3 Ni
4 Copper oxide
CHXI12:ORGANIC CHEMISTRY SOME BASIC PRINCIPLES AND TECHNIQUES

317523 \(0.257 \mathrm{~g}\) of an organic substance was heated with conc \(\mathrm{H}_{2} \mathrm{SO}_{4}\) and then distilled with excess of strong alkali. The ammonia gas evolved was absorbed in \({\rm{50}}\,\,{\rm{ml}}\) of \({\rm{N/10}}\,{\rm{HCl}}\) which required \({\rm{23}}{\rm{.2}}\,\,{\rm{ml}}\) of \({\rm{N/10}}\,\,{\rm{NaOH}}\) for neutralisation at the end of the process. The percentage of nitrogen in the compound is-

1 14.6
2 18.0
3 17.0
4 15.5
CHXI12:ORGANIC CHEMISTRY SOME BASIC PRINCIPLES AND TECHNIQUES

317524 Assertion :
The Duma's method is more appicable to nitrogen containing organic compounds than the Kjeldahl's method.
Reason :
The Kjeldahl's method does not give satisfactory results for compounds in which nitrogen is directly linked to oxygen.

1 Both Assertion and Reason are correct and Reason is the correct explanation of the Assertion.
2 Both Assertion and Reason are correct but Reason is not the correct explanation of the Assertion.
3 Assertion is correct but Reason is incorrect.
4 Assertion is incorrect but Reason is correct.
CHXI12:ORGANIC CHEMISTRY SOME BASIC PRINCIPLES AND TECHNIQUES

317525 During estimation of nitrogen present in an organic compound by Kjeldahl's method, the ammonia evolved from 0.5 g of the compound in Kjeldahl's estimation of nitrogen, neutralized 10 mL of \(1 \mathrm{M} \,\mathrm{H}_{2} \mathrm{SO}_{4}\). Find out the percentage of nitrogen in the compound.

1 \(53 \%\)
2 \(58 \%\)
3 \(56 \%\)
4 \(52 \%\)
CHXI12:ORGANIC CHEMISTRY SOME BASIC PRINCIPLES AND TECHNIQUES

317526 In Kjeldahl's method for the estimation of \(\mathrm{N}_{2}\), potassium sulphate and copper sulphate are used. On the basis of their functions which of the following statement(s) is/are correct?
(I) Potassium sulphate raises the b.pt. and ensures complete reaction.
(II) Copper sulphate acts as catalyst.
(III)Potassium sulphate acts as catalyst and copper sulphate raises the b.pt.

1 Only (III) is correct
2 (I) and (II) are correct
3 Only (II) is correct
4 None is correct
CHXI12:ORGANIC CHEMISTRY SOME BASIC PRINCIPLES AND TECHNIQUES

317522 In Dumas method for the estimation of \(\mathrm{N}_{2}\), the sample is heated with copper oxide and the gas evolved is passed over

1 Copper gauze
2 Pd
3 Ni
4 Copper oxide
CHXI12:ORGANIC CHEMISTRY SOME BASIC PRINCIPLES AND TECHNIQUES

317523 \(0.257 \mathrm{~g}\) of an organic substance was heated with conc \(\mathrm{H}_{2} \mathrm{SO}_{4}\) and then distilled with excess of strong alkali. The ammonia gas evolved was absorbed in \({\rm{50}}\,\,{\rm{ml}}\) of \({\rm{N/10}}\,{\rm{HCl}}\) which required \({\rm{23}}{\rm{.2}}\,\,{\rm{ml}}\) of \({\rm{N/10}}\,\,{\rm{NaOH}}\) for neutralisation at the end of the process. The percentage of nitrogen in the compound is-

1 14.6
2 18.0
3 17.0
4 15.5
CHXI12:ORGANIC CHEMISTRY SOME BASIC PRINCIPLES AND TECHNIQUES

317524 Assertion :
The Duma's method is more appicable to nitrogen containing organic compounds than the Kjeldahl's method.
Reason :
The Kjeldahl's method does not give satisfactory results for compounds in which nitrogen is directly linked to oxygen.

1 Both Assertion and Reason are correct and Reason is the correct explanation of the Assertion.
2 Both Assertion and Reason are correct but Reason is not the correct explanation of the Assertion.
3 Assertion is correct but Reason is incorrect.
4 Assertion is incorrect but Reason is correct.
CHXI12:ORGANIC CHEMISTRY SOME BASIC PRINCIPLES AND TECHNIQUES

317525 During estimation of nitrogen present in an organic compound by Kjeldahl's method, the ammonia evolved from 0.5 g of the compound in Kjeldahl's estimation of nitrogen, neutralized 10 mL of \(1 \mathrm{M} \,\mathrm{H}_{2} \mathrm{SO}_{4}\). Find out the percentage of nitrogen in the compound.

1 \(53 \%\)
2 \(58 \%\)
3 \(56 \%\)
4 \(52 \%\)
CHXI12:ORGANIC CHEMISTRY SOME BASIC PRINCIPLES AND TECHNIQUES

317526 In Kjeldahl's method for the estimation of \(\mathrm{N}_{2}\), potassium sulphate and copper sulphate are used. On the basis of their functions which of the following statement(s) is/are correct?
(I) Potassium sulphate raises the b.pt. and ensures complete reaction.
(II) Copper sulphate acts as catalyst.
(III)Potassium sulphate acts as catalyst and copper sulphate raises the b.pt.

1 Only (III) is correct
2 (I) and (II) are correct
3 Only (II) is correct
4 None is correct
CHXI12:ORGANIC CHEMISTRY SOME BASIC PRINCIPLES AND TECHNIQUES

317522 In Dumas method for the estimation of \(\mathrm{N}_{2}\), the sample is heated with copper oxide and the gas evolved is passed over

1 Copper gauze
2 Pd
3 Ni
4 Copper oxide
CHXI12:ORGANIC CHEMISTRY SOME BASIC PRINCIPLES AND TECHNIQUES

317523 \(0.257 \mathrm{~g}\) of an organic substance was heated with conc \(\mathrm{H}_{2} \mathrm{SO}_{4}\) and then distilled with excess of strong alkali. The ammonia gas evolved was absorbed in \({\rm{50}}\,\,{\rm{ml}}\) of \({\rm{N/10}}\,{\rm{HCl}}\) which required \({\rm{23}}{\rm{.2}}\,\,{\rm{ml}}\) of \({\rm{N/10}}\,\,{\rm{NaOH}}\) for neutralisation at the end of the process. The percentage of nitrogen in the compound is-

1 14.6
2 18.0
3 17.0
4 15.5
CHXI12:ORGANIC CHEMISTRY SOME BASIC PRINCIPLES AND TECHNIQUES

317524 Assertion :
The Duma's method is more appicable to nitrogen containing organic compounds than the Kjeldahl's method.
Reason :
The Kjeldahl's method does not give satisfactory results for compounds in which nitrogen is directly linked to oxygen.

1 Both Assertion and Reason are correct and Reason is the correct explanation of the Assertion.
2 Both Assertion and Reason are correct but Reason is not the correct explanation of the Assertion.
3 Assertion is correct but Reason is incorrect.
4 Assertion is incorrect but Reason is correct.
CHXI12:ORGANIC CHEMISTRY SOME BASIC PRINCIPLES AND TECHNIQUES

317525 During estimation of nitrogen present in an organic compound by Kjeldahl's method, the ammonia evolved from 0.5 g of the compound in Kjeldahl's estimation of nitrogen, neutralized 10 mL of \(1 \mathrm{M} \,\mathrm{H}_{2} \mathrm{SO}_{4}\). Find out the percentage of nitrogen in the compound.

1 \(53 \%\)
2 \(58 \%\)
3 \(56 \%\)
4 \(52 \%\)
CHXI12:ORGANIC CHEMISTRY SOME BASIC PRINCIPLES AND TECHNIQUES

317526 In Kjeldahl's method for the estimation of \(\mathrm{N}_{2}\), potassium sulphate and copper sulphate are used. On the basis of their functions which of the following statement(s) is/are correct?
(I) Potassium sulphate raises the b.pt. and ensures complete reaction.
(II) Copper sulphate acts as catalyst.
(III)Potassium sulphate acts as catalyst and copper sulphate raises the b.pt.

1 Only (III) is correct
2 (I) and (II) are correct
3 Only (II) is correct
4 None is correct
CHXI12:ORGANIC CHEMISTRY SOME BASIC PRINCIPLES AND TECHNIQUES

317522 In Dumas method for the estimation of \(\mathrm{N}_{2}\), the sample is heated with copper oxide and the gas evolved is passed over

1 Copper gauze
2 Pd
3 Ni
4 Copper oxide
CHXI12:ORGANIC CHEMISTRY SOME BASIC PRINCIPLES AND TECHNIQUES

317523 \(0.257 \mathrm{~g}\) of an organic substance was heated with conc \(\mathrm{H}_{2} \mathrm{SO}_{4}\) and then distilled with excess of strong alkali. The ammonia gas evolved was absorbed in \({\rm{50}}\,\,{\rm{ml}}\) of \({\rm{N/10}}\,{\rm{HCl}}\) which required \({\rm{23}}{\rm{.2}}\,\,{\rm{ml}}\) of \({\rm{N/10}}\,\,{\rm{NaOH}}\) for neutralisation at the end of the process. The percentage of nitrogen in the compound is-

1 14.6
2 18.0
3 17.0
4 15.5
CHXI12:ORGANIC CHEMISTRY SOME BASIC PRINCIPLES AND TECHNIQUES

317524 Assertion :
The Duma's method is more appicable to nitrogen containing organic compounds than the Kjeldahl's method.
Reason :
The Kjeldahl's method does not give satisfactory results for compounds in which nitrogen is directly linked to oxygen.

1 Both Assertion and Reason are correct and Reason is the correct explanation of the Assertion.
2 Both Assertion and Reason are correct but Reason is not the correct explanation of the Assertion.
3 Assertion is correct but Reason is incorrect.
4 Assertion is incorrect but Reason is correct.
CHXI12:ORGANIC CHEMISTRY SOME BASIC PRINCIPLES AND TECHNIQUES

317525 During estimation of nitrogen present in an organic compound by Kjeldahl's method, the ammonia evolved from 0.5 g of the compound in Kjeldahl's estimation of nitrogen, neutralized 10 mL of \(1 \mathrm{M} \,\mathrm{H}_{2} \mathrm{SO}_{4}\). Find out the percentage of nitrogen in the compound.

1 \(53 \%\)
2 \(58 \%\)
3 \(56 \%\)
4 \(52 \%\)
CHXI12:ORGANIC CHEMISTRY SOME BASIC PRINCIPLES AND TECHNIQUES

317526 In Kjeldahl's method for the estimation of \(\mathrm{N}_{2}\), potassium sulphate and copper sulphate are used. On the basis of their functions which of the following statement(s) is/are correct?
(I) Potassium sulphate raises the b.pt. and ensures complete reaction.
(II) Copper sulphate acts as catalyst.
(III)Potassium sulphate acts as catalyst and copper sulphate raises the b.pt.

1 Only (III) is correct
2 (I) and (II) are correct
3 Only (II) is correct
4 None is correct